Kaiser hosts a series of complimentary webinar presentations which demonstrate Raman Spectroscopy-based solutions. Hear from real customers and their success stories using Kaiser Raman analyzers and instruments. Examples of Research Raman, Analytical Raman, Process Raman, In Situ Raman, Industrial Raman, Remote Raman, and Raman Imaging and Microscopy are available during these sessions. We invite you to register for an upcoming webinar of interest, or view previous archives. Kaiser Webinar Archives are available in the sidebar -- see what you've been missing!
Real Customers - Their Applications, Raman Solutions
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Development of a Continuous Process for an Oxidative Nitration Reaction of a Nitroalkane
In this presentation, we will describe our approach for developing continuous processes, and present the application of this approach to an oxidative nitration reaction of a nitroalkane. We carried the product of oxidative nitration forward and reacted it with formaldehyde to form the corresponding 2,2-dinitroethanol derivative and isolated the product by means of a continuous pH adjustment. We will describe the advantages of performing data-rich experiments using automated lab reactors, collecting reaction calorimetry data, and using in situ Raman spectroscopy for this type of project, and present the results of a lab-scale demonstration of the continuous process with on-line Raman monitoring used as an in-process control to ensure acceptable product quality.
AIR DATE: March 31, 2016
Name: Dr. David Ford
Company: Nalas Engineering